HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyethanol → HCID 86630379, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyethanol | HCID 8019 | — |
| Reactant | N-(6-Chloro-4-oxo-1,4-dihydropyrido[3,2-d]pyrimidin-2-yl)acetamide | HCID 135978119 | — |
| Product | HCID 86630379 | HCID 86630379 | 14% |
Reaction Steps
5 mmol 2-acetamido-6-chloro-pyrido[3,2-d]pyrimidin-4(3H)-one (1.2 g) was reacted with 7.5 mmol 2-methoxyethanol (0.54 g) to give the pure title compound (0.2 g, yield: 14%) which was characterised as follows:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08232278B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-bfada9b13ec54629ae0826644f2d64a6 |
| Source note | uspto-grants-2012_07 |