HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86641267, compound → HCID 46196135, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86641267 | HCID 86641267 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 46196135 | HCID 46196135 | — |
Reaction Steps
step 7—A mixture of 128 (17 mg) and Pd(OH)2/C (20 mg) in EtOAc (10 mL) was stirred under 1 atm H2 for 30 min then the catalyst was filtered off. The filtrate was concentrated to afford 4.9 mg of I-90 as a waxy solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08232271B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-3df041ff62b841f9943fe1ccd5040199 |
| Source note | uspto-grants-2012_07 |