HCID 67168325, compound → HCID 58268550, compound

Participants

Reaction Steps

A mixture of A mixture of [1-[3-(methoxymethyl)-2-pyridyl]-3-methyl-pyrazol-4-yl]methanol (2.2 g, 9.4 mmol) and manganese (IV) oxide (19 g, 188.8 mmol) is stirred in dichloromethane (20 mL) at room temperature overnight. The reaction mixture is filtered over celite and the solvent evaporated under reduced pressure to yield 1.8 g of the title compound that is used without further purification. MS (m/z): 232 (M+1).

Provenance & Evidence