HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 52951552, compound → HCID 67168341, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 52951552 | HCID 52951552 | — |
| Reactant | HCID 58268556 | HCID 58268556 | — |
| Product | HCID 67168341 | HCID 67168341 | 32% |
Reaction Steps
This compound is essentially prepared as described in Preparation 7 by using 2-fluorospiro[4,5-dihydrothieno[2,3-c]pyran-7,4′-piperidine] and 2-(4-formyl-3-methyl-pyrazol-1-yl)pyridine-3-carbonitrile. The residue is purified by SCX to give 2-[4-[(2-fluorospiro[4,5-dihydrothieno[2,3-c]pyran-7,4′-piperidine]-1′-yl)methyl]-3-methyl-pyrazol-1-yl]pyridine-3-carbonitrile in a 32% yield. MS (m/z): 424 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08232289B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-1ffbe4e4491f4298a158d22a96cfe2a9 |
| Source note | uspto-grants-2012_07 |