HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 59334950, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 59334895 | HCID 59334895 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 59334950 | HCID 59334950 | — |
Reaction Steps
150 mg tert.butyl [(3,5-dichloro-phenylsulphonyl)-(2,3-dihydro-1H-indol-5-yl)-amino]-acetate are dissolved in 5 ml dichloromethane. 110 mg potassium carbonate and 45 μl benzoyl chloride are added, the mixture is stirred for 3 hours at ambient temperature and then divided between dichloromethane and water. The organic phase is washed with water and then dried on magnesium sulphate. The solvents are eliminated in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08232312B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-6802d6dcd4e14ab7bbe5885bd58bce19 |
| Source note | uspto-grants-2012_07 |