Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonia → 1-Chloro-3-methoxy-5-nitrobenzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonia | HCID 222 | — |
| 반응물 | Dimethyl Sulfate | HCID 6497 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 3-Chloro-5-nitrophenol | HCID 10675815 | — |
| 용매 | Ethanol | HCID 702 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 1-Chloro-3-methoxy-5-nitrobenzene | HCID 14026050 | — |
반응 단계
10 g 3-chloro-5-nitrophenol are dissolved in 250 ml of ethanol. 11.9 g potassium carbonate and 6 ml dimethylsulphate are added and the mixture is stirred for 12 hours at ambient temperature. Then 3 ml of a 33% ammonia solution are added and then the ethanol is eliminated in vacuo. The residue is taken up in water and the precipitated solid is suction filtered and dried.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08232312B2 |
| 출처 데이터셋 | uspto-grants-2012_07 |
| ORD ID | ord-33e31a16b14943b5bb5a4413f4a8bae3 |
| 출처 메모 | uspto-grants-2012_07 |