HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Nitro-benzo[b]thiophene-3-carboxylic acid → 5-Nitro-3-benzothiophencarboxylic acid amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Nitro-benzo[b]thiophene-3-carboxylic acid | HCID 23504836 | — |
| Reactant | 6-Nitro-benzo[b]thiophene-3-carboxylic acid | HCID 59335110 | — |
| Product | 5-Nitro-3-benzothiophencarboxylic acid amide | HCID 57091576 | — |
Reaction Steps
are obtained as a mixture during the reaction of a mixture of 6-nitro-benzo[b]-thiophene-3-carboxylic acid and 5-nitro-benzo[b]thiophene-3-carboxylic acid (Example XLV). The crude product is chromatographed on silica gel, while the two products are obtained as a mixture and further reacted directly in Example XII (30).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08232312B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-eeebebb11f37485ab533471d5c34c788 |
| Source note | uspto-grants-2012_07 |