HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorophenylboronic acid → HCID 178478011, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorophenylboronic acid | HCID 2734322 | — |
| Reactant | HCID 178419324 | HCID 178419324 | — |
| Product | HCID 178478011 | HCID 178478011 | — |
Reaction Steps
The title compound was prepared from 3-(5-bromo-1H-benzimidazol-2-yl)-1-oxa-2-aza-spiro[4.5]dec-2-ene (as prepared in the previous step) and 2-chloro-benzene-boronic acid according to the procedure described in Example 1, step D. 1H-NMR (400 MHz, d4-MeOH) δ: 7.46-7.76 (m, 3H), 7.29-7.42 (m, 4H), 3.27 (s, 2H), 1.69-1.87 (m, 6H), 1.46-1.62 (m, 4H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08232409B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-9ef74b1ae94d4af1a56e0fa8f2a1b833 |
| Source note | uspto-grants-2012_07 |