HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 59447532, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 59447599 | HCID 59447599 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59447532 | HCID 59447532 | — |
Reaction Steps
Compound 57B (40 mg, 0.131 mmol) in MeOH (3 ml) was treated with 2 N hydrogen chloride in ether (0.1 ml, 0.200 mmol) for 1 h and the mixture was concentrated to provide the title compound 57C. LCMS (APCI) m/e 177 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08232273B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-fba4d7d9315c49bb8691e20fbfe59f61 |
| Source note | uspto-grants-2012_07 |