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HRID1518372

反应详情

EQUATION

反应方程式

HRID 1518372 的结构方程式

REACTANTS

反应物

4
结构：c1ccc(N2CCNCC2)cc1
HCID7096

Phenylpiperazine

C10H14N2

结构：Oc1cccc(N2CCNCC2)c1
HCID2736597

1-(3-Hydroxyphenyl)piperazine

C10H14N2O

结构：COC(=O)c1nc(N2CCc3cccc(C(=O)N(COCC[Si](C)(C)C)c4nc5ccccc5s4)c3C2)sc1CN1CCN(c2ccccc2)CC1
HCID59447670

未命名化合物

结构：COC(=O)c1nc(N2CCc3cccc(C(=O)/N=c4/sc5ccccc5n4COCC[Si](C)(C)C)c3C2)sc1C=O
HCID178499107

未命名化合物

PRODUCTS

生成物

1
结构：CN1CCN(c2cccc(O)c2)CC1
HCID11011455

3-(4-methylpiperazin-1-yl)phenol

C11H16N2O

PROCEDURE

实验过程

Compound 87A was prepared in a similar manner to the synthesis of compound 62A by substituting compound 45C and phenylpiperazine with paraformahyde and 3-(piperazin-1-yl)phenol, respectively: 1H NMR (DMSO-d6): δ 9.07 (s, 1H), 6.94-6.98 (m, 1H), 6.36 (d, J=8.13, 2.4 Hz, 2H), 8.28-8.29 (m, 1H), 6.18-6.21 (m, 1H), 3.04-3.07 (m, 4H), 2.41-2.43 (m, 4H), 2.21 (s, 3H). ESI (+)/MS: 193 (M+H)+.