HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14343212, compound → HCID 12637757, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14343212 | HCID 14343212 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 12637757 | HCID 12637757 | — |
Reaction Steps
A mixture of 4-methyl-2-phenylethynyl-pyridine (18.2 g) and 10% palladium on carbon (2.0 g) in methanol (300 mL) is stirred under hydrogen atmosphere (50 psi) at ambient temperature until the triple bond is completely reduced (20 h). The mixture is filtrered and the solvent is removed under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09073870B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-1623e21499c743de8240c667b9214958 |
| Source note | uspto-grants-2015_07 |