HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-4-methylthiophene-3-carboxamide → HCID 68786937, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-4-methylthiophene-3-carboxamide | HCID 293810 | — |
| Reactant | HCID 13569193 | HCID 13569193 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 68786937 | HCID 68786937 | — |
Reaction Steps
This compound was prepared from 2-(4-(2-(1H-imidazol-1-yl)ethoxy)phenyl)acetic acid and 2-amino-4-methylthiophene-3-carboxamide using protocol B except that triethylamine was also added. The crude product was purified via silica gel column chromatography. Method[1], MS(ESI) 385.1, Retention time=1.254 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09073891B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-4a3294dbb7b3419d906adb01da7303c1 |
| Source note | uspto-grants-2015_07 |