HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-3-nitrothiophene → HCID 68754289, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-3-nitrothiophene | HCID 220186 | — |
| Reactant | 2-(Tributylstannyl)-1,3-thiazole | HCID 2763259 | — |
| Reactant | HCID 68754289 | HCID 68754289 | — |
| Product | HCID 68754289 | HCID 68754289 | — |
| Product | HCID 68754843 | HCID 68754843 | — |
Reaction Steps
2-(3-Nitrothiophen-2-yl)thiazole was synthesized from 2-chloro-3-nitrothiophene according to protocol E except that 2-(tributylstannyl)thiazole was used. Method[1], MS(ESI) 212.9 [M+H], Retention time=2.163 min. 2-(Thiazol-2-yl)thiophen-3-amine was synthesized from 2-(3-nitrothiophen-2-yl)thiazole according to protocol F. Method[1], MS(ESI) 183 [M+H], Retention time=1.718 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09073891B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-7bd1335ace894cdb8585f2686956c0a7 |
| Source note | uspto-grants-2015_07 |