HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Naphthaleneacetic Acid → Methyl 3-(2-(naphthalen-1-yl)acetamido)thiophene-2-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Naphthaleneacetic Acid | HCID 6862 | — |
| Reactant | Methyl 3-amino-2-thiophenecarboxylate | HCID 89652 | — |
| Product | Methyl 3-(2-(naphthalen-1-yl)acetamido)thiophene-2-carboxylate | HCID 25660569 | — |
Reaction Steps
Methyl 3-(2-(naphthalen-1-yl)acetamido)thiophene-2-carboxylate was prepared from methyl 3-aminothiophene-2-carboxylate (4.30 g, 27.3 mmol) and 2-(naphthalen-1-yl)acetic acid (3.10 g, 27.3 mmol) according to protocol A. Retention time (min)=8.738, method [7], MS(ESI) 326.1 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09073891B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-85d3cbb778b242d68a676936a99d5b1e |
| Source note | uspto-grants-2015_07 |