HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 136931791, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 135465814 | HCID 135465814 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 136931791 | HCID 136931791 | 93.4% |
Reaction Steps
Dissolve ethyl 2-methyl-6-oxo-1H-pyrimidine-4-carboxylate (7.26 g, 39.9 mmol) in a solution of ammonia in MeOH (70 mL, 7 N) and stir the mixture for 17 hours at ambient temperature. Remove the solvents under reduced pressure to provide the title compound as a black solid (5.7 g, 93.4%). MS (m/z): 154 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09073901B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-8ade013e3b83427f80080b892412e3e2 |
| Source note | uspto-grants-2015_07 |