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HRID1520599

反应详情

EQUATION

反应方程式

HRID 1520599 的结构方程式

REACTANTS

反应物

3
结构：O=S(=O)(Cl)c1ccccc1
HCID7369

Benzenesulfonyl chloride

C6H5ClO2S

结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：NS(=O)(=O)c1ccc(NC2CCNCC2)c([N+](=O)[O-])c1
HCID43345806

未命名化合物

PRODUCTS

生成物

1
结构：NS(=O)(=O)c1ccc(NC2CCN(S(=O)(=O)c3ccccc3)CC2)c([N+](=O)[O-])c1
HCID68407000

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

A mixture of EXAMPLE 157B (84 mg), benzenesulfonyl chloride (46 mg), and triethylamine (101 mg) in CH2Cl2 (2 mL) was stirred for 1 hours. The product was chromatographed on silica gel with 25% ethyl acetate/hexanes.

WORKUP

后处理

  1. customThe product was chromatographed on silica gel with 25% ethyl acetate/hexanes