Phosphorus oxychloride → HCID 86686086, compound

HRID 1520751Notes

Reaction equation

HRID 1520751 reaction equation
[CH:1]1[C:6]2[NH:7][C:8](=O)[C:9]3[C:10]4[CH:19]=[CH:18][CH:17]=[CH:16][C:11]=4[C:12](=[O:15])[NH:13][C:14]=3[C:5]=2[CH:4]=[CH:3][CH:2]=1.O=P(Cl)(Cl)[Cl:23]>>[Cl:23][C:8]1[N:7]=[C:6]2[CH:1]=[CH:2][CH:3]=[CH:4][C:5]2=[C:14]2[C:9]=1[C:10]1[CH:19]=[CH:18][CH:17]=[CH:16][C:11]=1[C:12](=[O:15])[NH:13]2

Participants

3

Reactant 2

HCID 24813Phosphorus oxychlorideHCID 86686087HCID 86686087, compound

Product 1

HCID 86686086HCID 86686086, compound

Procedure

chlorinating a dibenzo[c,h][1,6]naphthyridine-6,11(5H,12H)-dione with a chlorinating reagent comprising POCl3 to give the corresponding 11-chlorodibenzo[c,h][1,6]-naphthyridin-6(5H)-one; and/or

Sources & evidence

ORD record
ord-becdf1d2f761444abbf8158622dc9ea3
Source dataset
uspto-grants-2015_07
Patent number
US09073920B2

Reaction notes

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