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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1522450Generated: October 30, 2026

Sodium Hydroxide → HCID 67124654, compound

https://huagongshe.com/reaction/1522450

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium HydroxideHCID 14798—
ReactantHCID 68078899HCID 68078899—
SolventEthanolHCID 702—
ProductHCID 67124654HCID 67124654—

Reaction Steps

The title compound was prepared in the same manner as described for intermediate 46 using ethyl 6-cyclopropyl-1-(4-pyridinyl)-3-methyl-1H-pyrazolo[3,4-b]pyridine-4-carboxylate (240 mg, 0.796 mmol), sodium hydroxide (4 mL, 4.00 mmol), and ethanol (30 mL), wherein the stir time was 1 h. The final product was collected as 0.210 g (89%). LCMS E-S (M+H)=295.3.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09073924B2
Source datasetuspto-grants-2015_07
ORD IDord-54c43a884d7240f585123617c7ed28af
Source noteuspto-grants-2015_07