HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dibromobutane → 1-Pyrrolidineethanol,beta-methyl-,(betaR)-(9CI)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dibromobutane | HCID 8056 | — |
| Reactant | (R)-(-)-2-Amino-1-propanol | HCID 80308 | — |
| Product | 1-Pyrrolidineethanol,beta-methyl-,(betaR)-(9CI) | HCID 15203027 | — |
Reaction Steps
The title compound was synthesized as described in Intermediate 9 using 1,4-dibromobutane and (R)-2-aminopropan-1-ol as starting materials. 1H NMR (CDCl3): δ 3.61 (m, 1H), 3.38 (m, 1H), 2.97 (br s, 1H), 2.72 (m, 1H), 2.60 (br s, 4H), 1.78 (br s, 4H), 1.06 (d, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09078871B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-f76d370ce6914fc7a98bf6b586ca4616 |
| Source note | uspto-grants-2015_07 |