HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → N-phenyl-N-(4-phenylphenyl)-N-(9-phenyl-9H-carbazol-3-yl)amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | N-phenyl-(1,1'-biphenyl)-4-amine | HCID 13087229 | — |
| Reactant | 3-Bromo-9-phenylcarbazole | HCID 18942624 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | N-phenyl-N-(4-phenylphenyl)-N-(9-phenyl-9H-carbazol-3-yl)amine | HCID 71059317 | — |
Reaction Steps
The Rf values of the objective substance, 3-bromo-9-phenyl-9H-carbazole, and N-phenyl-N-(4-phenylphenyl)amine were respectively 0.65, 0.73, and 0.54, which were obtained by silica gel thin layer chromatography (TLC) (with a developing solvent containing ethyl acetate and hexane in a 1:5 ratio).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09079855B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-47fc3921fefd422ebef6b626a2d88847 |
| Source note | uspto-grants-2015_07 |