HRID1523

反应详情

EQUATION

反应方程式

HRID 1523 的结构方程式

PROCEDURE

实验过程

A solution of (R)-3-(3,4-dimethoxyphenyl)-2-propylamine hydrochloride1 (500 mg, 2.15 mMol) in hydrogen bromide (48%, 5 ml) was stirred at 100° C. under an argon atmosphere for 20 hours. After cooling, the solvent was evaporated and the residue was dried giving the title compound.

WORKUP

后处理

  1. temperatureAfter cooling
  2. customthe solvent was evaporated
  3. customthe residue was dried