HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
5-chloro-1H-indole-2,3-dione → 5-Chloro-1-(2-(piperidin-1-yl)ethyl)indoline-2,3-dione
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 5-chloro-1H-indole-2,3-dione | HCID 87203 | — |
| Edukt | 1-(2-Bromoethyl)piperidine | HCID 426611 | — |
| Edukt | 1-propyl-1H-indole-2,3-dione | HCID 1645090 | — |
| Produkt | 5-Chloro-1-(2-(piperidin-1-yl)ethyl)indoline-2,3-dione | HCID 8071686 | — |
Reaktionsschritte
Was prepared in an analogous manner to 1-propylindoline-2,3-dione using commercially available 5-chloroisatin (purchased from Fisher Scientific) and 1-(2-bromoethyl)piperidine (purchased from Fisher Scientific). 1H-NMR δ 7.55 (m, 2H), 6.95 (d, 1H), 3.84 (t, 2H), 2.58 (t, 2H), 2.46 (bs, 4H), 1.54 (m, 4H), 1.43 (m, 2H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09079853B2 |
| Quelldatensatz | uspto-grants-2015_07 |
| ORD ID | ord-738afd8c297b482d9b46f0c2e7edc803 |
| Quellennotiz | uspto-grants-2015_07 |