HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Ethyl-5-methyl-2-oxo-3-(3,4,5-trimethoxybenzyl)indolin-3-yl benzoate → 1-Isobutyl-2-oxo-3-(3,4,5-trimethoxybenzyl)indolin-3-yl benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Ethyl-5-methyl-2-oxo-3-(3,4,5-trimethoxybenzyl)indolin-3-yl benzoate | HCID 86300681 | — |
| Reactant | 1-Isobutyl-2-oxoindolin-3-yl benzoate | HCID 90417901 | — |
| Product | 1-Isobutyl-2-oxo-3-(3,4,5-trimethoxybenzyl)indolin-3-yl benzoate | HCID 86300968 | — |
Reaction Steps
This compound was made in an analogous fashion to 1-ethyl-5-methyl-2-oxo-3-(3,4,5-trimethoxybenzyl)indolin-3-yl benzoate using 1-isobutyl-2-oxoindolin-3-yl benzoate. 1H-NMR δ 8.05 (d, 2H), 7.57 (dd, 1H), 7.43 (dd, 2H), 7.27 (m, 1H), 7.17 (d, 1H), 7.01 (dd, 1H), 6.73 (d, 1H), 6.17 (2H), 3.78 (s, 3H), 3.66 (s, 6H), 3.51 (m, 2H), 3.25 (m, 2H), 1.97 (m, 1H), 0.82 (dd, 6H). Calculated mass for C29H31NO6, 489.22. Observed 512.3 (M+Na).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09079853B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-3a0c1019ff754d5ba1370a86d632703d |
| Source note | uspto-grants-2015_07 |