HCID 68779648, compound → HCID 59627200, compound

Participants

Reaction Steps

The title compound was prepared from (R)-4-allyl-1-((S)-1-cyclohexylethyl)-3-methyl-4-phenyltetrahydropyrimidin-2(1H)-one following a procedure analogous to that described in Example 7. (R)-4-allyl-1-((S)-1-cyclohexylethyl)-3-methyl-4-phenyltetrahydropyrimidin-2(1H)-one was prepared from (R)-4-allyl-1-((S)-1-cyclohexylethyl)-4-phenyltetrahydropyrimidin-2(1H)-one following a procedure analogous to that described in Example 3. LC-MS Method 2 tR=1.408 min, m/z=359.1; 1H NMR (CDCl3) δ=1.06 (m, 3H), 1.10 (m, 3H), 1.23 (m, 3H), 1.52 (m, 7H), 1.75 (m, 2H), 1.98 (m, 1H), 2.15 (m, 2H), 2.60 (m, 1H), 2.87 (m, 3H), 3.70 (m, 2H), 4.22 (m, 11-1), 7.17 (m, 4H), 7.28 (m, 2H).

Provenance & Evidence