HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boronic acid, B-(2-(((1,1-dimethylethyl)amino)sulfonyl)phenyl)- → HCID 90313766, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boronic acid, B-(2-(((1,1-dimethylethyl)amino)sulfonyl)phenyl)- | HCID 4997616 | — |
| Reactant | 1-(4-Bromo-2-fluorophenyl)ethan-1-one | HCID 21938581 | — |
| Product | HCID 90313766 | HCID 90313766 | — |
Reaction Steps
The title compound was prepared using conditions analogous to those described in Example 1 using (2-(N-(tert-butyl)sulfamoyl)phenyl)boronic acid and 1-(4-bromo-2-fluorophenyl)ethanone. 1H NMR (500 MHz, CDCl3) δ 8.19 (dd, J=7.9, 1.3, 1H), 7.95 (m, 1H), 7.63-7.57 (m, 1H), 7.57-7.52 (m, 1H), 7.38-7.30 (m, 2H), 7.28 (dd, J=7.5, 1.3, 1H), 2.70 (d, J=4.9, 3H), 1.05 (m, 9H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09079866B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-b31e70f2708645c7810ad6a555a85169 |
| Source note | uspto-grants-2015_07 |