HRID1524104

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID11358

Benzene, 1-bromo-2-methoxy-

C7H7BrO

结构：CC1(C)OB(c2ccc(-c3cnc(N)nc3)nc2)OC1(C)C

HCID90314121

5-[5-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-2-pyridinyl]-2-pyrimidinamine

C15H19BN4O2

PRODUCTS

生成物

HCID90313849

未命名化合物

PROCEDURE

实验过程

The title compound was prepared in a manner similar to that described in Example 427 using 5-(5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-yl)pyrimidin-2-amine and 1-bromo-2-methoxybenzene. MS (ESI): mass calcd. for C16H14N4O. C2HF3O2, 278.12; m/z found, 279.1 [M+H]+. 1H NMR (400 MHz, CD3OD) δ 9.00 (s, 2H), 8.81 (d, J=2.2, 1H), 8.28 (dd, J=8.4, 2.2, 1H), 8.02 (d, J=8.4, 1H), 7.48-7.41 (m, 2H), 7.16 (d, J=8.4, 1H), 7.11 (m, 1H), 3.87 (s, 3H).