HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → (3-Methyl-but-3-enyloxymethyl)-benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Product | (3-Methyl-but-3-enyloxymethyl)-benzene | HCID 11095166 | — |
Reaction Steps
BnBr was added to the mixture of alcohol and NaH in DMF cooled in an ice bath. The mixture was stirred at room temperature overnight and the solid was filtered. The solvent was removed and the residue was purified by column chromatography to give compound 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09079913B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-e42ca219eeba496a90ffe45b2200bcfc |
| Source note | uspto-grants-2015_07 |