Hydroxyamine hydrochloride → HCID 89470836, compound

Participants

Reaction Steps

To a solution of compound 38-c (530 mg, 2.5 mmol) in ethanol (10 mL) was added hydroxylamine hydrochloride (230 mg, 3.2 mmol) and NaHCO3 (360 g, 3.60 mmol). The reaction mixture was then stirred for 10 h at room temperature. The resulting mixture was concentrated under reduce pressure to afford crude compound 38-d (570 mg). LC-MS 228 [M+H]+

Provenance & Evidence