Cyclopropylacetylene → HCID 90391022, compound

HRID 1526614Notes

Reaction equation

[C:1]([C:4]1[CH:5]=[N:6][NH:7][CH:8]=1)#[C:2][CH3:3].[CH:9]1(C#C)C[CH2:10]1>>[CH:3]1([C:2]#[C:1][C:4]2[CH:5]=[N:6][NH:7][CH:8]=2)[CH2:10][CH2:9]1

Participants

Reactant 2

HCID 138823Cyclopropylacetylene

HCID 57090177HCID 57090177, compound2×

Product 1

HCID 90391022HCID 90391022, compound

Procedure

The title compound was synthesized according to the procedure described for 4-(prop-1-yn-1-yl)-1H-pyrazole (intermediate 61) above, but using cyclopropylacetylene. LC/MS (ESI−) m/z=133.1 (M+H).

Sources & evidence

ORD record: ord-ecfd70babf414b3b830c3562a7bfe65f
Source dataset: uspto-grants-2015_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09085576B2

Reaction notes

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