Tetrahydrofuran → HCID 178506925, compound

HRID 1526760Notes

Reaction equation

[CH2:1]([NH:5][CH2:6][CH2:7][CH2:8][CH3:9])[CH2:2][CH2:3][CH3:4].C([Li:14])CCC.O1CCCC1>>[CH2:1]([N:5]([Li:14])[CH2:6][CH2:7][CH2:8][CH3:9])[CH2:2][CH2:3][CH3:4]

Participants

Reactant 3

HCID 8028Tetrahydrofuran

HCID 8148Dibutylamine

HCID 178418339Butyllithium

Product 1

HCID 178506925HCID 178506925, compound

Procedure

As a polymerization initiator, dibutylamine (13.0 mmol) and n-butyllithium (13.0 mmol) were previously reacted in the presence of tetrahydrofuran (26.0 mmol) to obtain dibutylamino lithium. A cyclohexane solution of dibutylamino lithium (13.0 mmol) was supplied to the reactor.

Sources & evidence

ORD record: ord-0ff0b43d217a4f51bc19f9dbb54d0891
Source dataset: uspto-grants-2015_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09085653B2

Reaction notes

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