Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Benzyl bromoacetate | HCID 62576 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 85615786 | HCID 85615786 | — |
Reaction Steps
To a solution of benzyl bromoacetate (10 g, 43.7 mmol) in acetone (200 mL) was added a solution of pyridine (3.51 mL, 43.7 mmol) in acetone (20 mL) and the resulting mixture was stirred at 60° C. under nitrogen over the week-end. Then allowed to cool to RT and concentrated to give the desired material. MS (LC/MS): 228.1 [MH]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09085555B2 |
|---|
| Source dataset | uspto-grants-2015_07 |
|---|
| ORD ID | ord-9c6eeac9948e41bfac2e9a2d61ae7571 |
|---|
| Source note | uspto-grants-2015_07 |
|---|
