HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
(1-Carbamoyl-1H-indol-3-yl)-acetic acid → (1-Carbamoyl-2-methyl-1H-indol-3-yl)-acetic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | (1-Carbamoyl-1H-indol-3-yl)-acetic acid | HCID 68283440 | — |
| Edukt | (1-carbamoyl-2-methyl-1H-indol-3-yl)-acetic acid ethyl ester | HCID 68283853 | — |
| Produkt | (1-Carbamoyl-2-methyl-1H-indol-3-yl)-acetic acid | HCID 68283651 | — |
Reaktionsschritte
was prepared in a similar manner as described in Scheme A8 Step B for (1-carbamoyl-1H-indol-3-yl)-acetic acid starting from (1-carbamoyl-2-methyl-1H-indol-3-yl)-acetic acid ethyl ester. The crude product (brownish solid) obtained after extractive work-up was used directly in the next step without purification. MS: 233 [M+H]+; tR (HPLC conditions b) 3.26 min.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09085555B2 |
| Quelldatensatz | uspto-grants-2015_07 |
| ORD ID | ord-7b80917c3ce84bc49582c0dbcecfb519 |
| Quellennotiz | uspto-grants-2015_07 |