Hydrochloric Acid → HCID 131733206, compound

Participants

Reaction Steps

To a solution of [3-chloro-2-fluoro-5-(2H-tetrazol-5-yl)-benzyl]-carbamic acid tert-butyl ester (1.06 g, 3.23 mmol) in dioxane (20 mL) was added a 4M HCl solution in dioxane (8.09 mL, 32.3 mmol). The reaction mixture was stirred at RT for 72 h and then freeze-dried overnight to afford the title compound as a white solid. MS (LC/MS): 228.0 [M+H]+; tR (HPLC conditions c): 2.68 min.

Provenance & Evidence