HRID1527691

反应详情

EQUATION

反应方程式

REACTANTS

反应物

$结构：COc1cc(/C=C(\C)C(=O)O)c(OC)c2ccccc12$

HCID46180242

未命名化合物

$结构：CCC/C(=C\c1c(Br)c(OC)c2ccccc2c1OC)C(=O)OCC$

HCID86647737

未命名化合物

PRODUCTS

生成物

$结构：CCC/C(=C\c1c(Br)c(OC)c2ccccc2c1OC)C(=O)O$

HCID68770455

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

Compound 99f was prepared from 98f (0.177 g, 0.435 mmol) as described above for 29a to give 0.078 g (0.21 mmol, 47%) of the product as a white solid following flash chromatography (1:3 EtOAc:hexanes 0.5% AcOH) and recrystallization from Et2O/hexanes.

WORKUP

后处理

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