HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 46180046, compound → HCID 46180314, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 46180046 | HCID 46180046 | — |
| Reactant | (E)-3-(1,4-dimethoxynaphthalen-2-yl)-2-methylpropenoic acid | HCID 46180242 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 46180314 | HCID 46180314 | — |
Reaction Steps
Compound 99g was prepared from 98g (0.073 g, 0.22 mmol) as described above for 29a to give 0.068 g (0.22 mmol, 100%) of the product as a tan solid following flash chromatography (1:3 EtOAc:hexanes 0.5% AcOH) and recrystallization from Et2O/hexanes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09089605B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-536db8ccef6346b3aeed7e3d929240f6 |
| Source note | uspto-grants-2015_07 |