HRID1527692

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CCOC(=O)/C(C)=C/c1c(OC)c(OC)c2ccccc2c1OC

HCID46180046

未命名化合物

$结构：COc1cc(/C=C(\C)C(=O)O)c(OC)c2ccccc12$

HCID46180242

未命名化合物

PRODUCTS

生成物

$结构：COc1c(/C=C(\C)C(=O)O)c(OC)c2ccccc2c1OC$

HCID46180314

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

Compound 99g was prepared from 98g (0.073 g, 0.22 mmol) as described above for 29a to give 0.068 g (0.22 mmol, 100%) of the product as a tan solid following flash chromatography (1:3 EtOAc:hexanes 0.5% AcOH) and recrystallization from Et2O/hexanes.

WORKUP

后处理

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