HRID1527696

反应详情

EQUATION

反应方程式

REACTANTS

反应物

$结构：C/C(=C\C1=CC(=O)c2ccccc2C1=O)C(=O)O$

HCID25235423

未命名化合物

$结构：COc1c(C)c(/C=C(\C)C(=O)O)c(OC)c2ccccc12$

HCID46180244

未命名化合物

PRODUCTS

生成物

$结构：CC1=C(/C=C(\C)C(=O)O)C(=O)c2ccccc2C1=O$

HCID25235424

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

Compound 35a was prepared from 99a (0.083 g, 0.29 mmol) as described above for 30a to give 0.048 g (0.19 mmol, 65%) of the product as a yellow solid following flash chromatography (3:17 acetone:hexanes 0.5% AcOH) and recrystallization from Et2O/hexanes.

WORKUP

后处理

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