HRID1527697

反应详情

EQUATION

反应方程式

REACTANTS

反应物

$结构：C/C(=C\C1=CC(=O)c2ccccc2C1=O)C(=O)O$

HCID25235423

未命名化合物

$结构：CCCC/C(=C\c1c(C)c(OC)c2ccccc2c1OC)C(=O)O$

HCID68769894

未命名化合物

PRODUCTS

生成物

$结构：CCCC/C(=C\C1=C(C)C(=O)c2ccccc2C1=O)C(=O)O$

HCID25235470

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID3283

Diethyl Ether

C4H10O

PROCEDURE

实验过程

Compound 35b was prepared from 99b (0.148 g, 0.45 mmol) as described above for 30a to give 0.050 g (0.17 mmol, 37%) of the product as a yellow solid following flash chromatography (2:3 Et2O:hexanes 0.5% AcOH) and recrystallization from Et2O/hexanes.

WORKUP

后处理

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