HRID1527699

反应详情

EQUATION

反应方程式

REACTANTS

反应物

$结构：C/C(=C\C1=CC(=O)c2ccccc2C1=O)C(=O)O$

HCID25235423

未命名化合物

$结构：COc1c(/C=C(\C)C(=O)O)c(SC)c(OC)c2ccccc12$

HCID46180316

未命名化合物

PRODUCTS

生成物

$结构：COC1=C(/C=C(\C)C(=O)O)C(=O)c2ccccc2C1=O$

HCID25235468

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID3283

Diethyl Ether

C4H10O

PROCEDURE

实验过程

Compound 55 was prepared from 99h (0.180 g, 0.565 mmol) as described above for 30a to give 0.063 g (0.22 mmol, 38%) of the product as a red fluffy solid following flash chromatography (2:3 Et2O:hexanes 0.5% AcOH) and recrystallization from Et2O/hexanes.

WORKUP

后处理

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