HRID1527705

反应详情

EQUATION

反应方程式

REACTANTS

反应物

$结构：C/C(=C\C1=C(Br)C(=O)c2ccccc2C1=O)C(=O)O$

HCID25235467

未命名化合物

$结构：COc1c(Cl)c(/C=C(\C)C(=O)O)c(OC)c2ccccc12$

HCID46180319

未命名化合物

PRODUCTS

生成物

$结构：C/C(=C\C1=C(Cl)C(=O)c2ccccc2C1=O)C(=O)O$

HCID25235426

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

Compound 43a was prepared from 42a (0.872 g, 2.84 mmol) as described above for 39a to give 0.121 g (0.437 mmol, 16%) of the product as a yellow solid following flash chromatography (2:3 acetone:hexanes 0.5% AcOH) and recrystallization from Et2O/hexanes. (0.121 g E; 0.115 g Z methyl ester)

WORKUP

后处理

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