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HRID1528018

反应详情

EQUATION

反应方程式

HRID 1528018 的结构方程式

REACTANTS

反应物

2
结构：CC1=CC(=O)c2ccccc2C1=O
HCID4055

Menadione

C11H8O2

结构：CC(C)(C)OC(=O)Nc1ccc(CC(=O)O)cc1
HCID2824993

{4-[(tert-Butoxycarbonyl)amino]phenyl}acetic acid

C13H17NO4

PRODUCTS

生成物

1
结构：CC1=C(Cc2ccc(NC(=O)OC(C)(C)C)cc2)C(=O)C2C=CC=CC2C1=O
HCID67057807

未命名化合物

收率 12%

PROCEDURE

实验过程

As starting materials for the coupling reaction menadione and (4-tert-Butoxycarbonylamino-phenyl)-acetic acid were used. Synthesis is realized according to the general procedure described in general procedure of example 1. After chromatography on silica gel (cyclohexane:ethyl acetate=3:1, UV), 527 mg (1.4 mmol, 12% yield) of P_TM45 were isolated as yellow solid.

WORKUP

后处理

  1. customSynthesis