HuagongsheHuagongshe Chemistry Print Report · For research reference only
Menadione → HCID 67057807, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Menadione | HCID 4055 | — |
| Reactant | 2-(4-((Tert-butoxycarbonyl)amino)phenyl)acetic acid | HCID 2824993 | — |
| Product | HCID 67057807 | HCID 67057807 | 12% |
Reaction Steps
As starting materials for the coupling reaction menadione and (4-tert-Butoxycarbonylamino-phenyl)-acetic acid were used. Synthesis is realized according to the general procedure described in general procedure of example 1. After chromatography on silica gel (cyclohexane:ethyl acetate=3:1, UV), 527 mg (1.4 mmol, 12% yield) of P_TM45 were isolated as yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09090549B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-17fbc7e633664ae5aed089ffd2b32b25 |
| Source note | uspto-grants-2015_07 |