HuagongsheHuagongshe Chemistry Print Report · For research reference only
Menadione → HCID 67057796, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Menadione | HCID 4055 | — |
| Reactant | 4-Isopropylphenylacetic acid | HCID 78230 | — |
| Product | HCID 67057796 | HCID 67057796 | 58% |
Reaction Steps
As starting materials for the coupling reaction menadione and 4-isopropylphenylacetic acid were used. Synthesis is realized according to the general procedure described in general procedure of example 1. After chromatography on silica gel (petroleum ether:CH2Cl2=1:1, UV), 395 mg (1.30 mmol, 58% yield) of P_TM100 were isolated as yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09090549B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-b42bbdeaf1c743a5a67897f2401705f0 |
| Source note | uspto-grants-2015_07 |