HuagongsheHuagongshe Chemistry Print Report · For research reference only
Menadione → HCID 67057787, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Menadione | HCID 4055 | — |
| Reactant | 2-Bromo-4-methoxyphenylacetic acid | HCID 3963668 | — |
| Product | HCID 67057787 | HCID 67057787 | 57% |
Reaction Steps
As starting materials for the coupling reaction menadione and 2-Bromo-4-methoxyphenylacetic acid were used. Synthesis is realized according to the general procedure described in general procedure of example 1. After chromatography on silica gel (petroleum ether:CH2Cl2=1:1, UV), 857 mg (2.31 mmol, 57% yield) of P_TM102 were isolated as yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09090549B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-c3cb222614f94c5abf59bb1144230a8d |
| Source note | uspto-grants-2015_07 |