m-Chloroperbenzoic acid → HCID 68014666, compound

Participants

Reaction Steps

To a DMF solution (2.0 ml) of m-chloroperbenzoic acid (0.398 mg) was added a DMF solution (12.0 ml) of 5-methoxy-3-(1-phenyl-1H-pyrazol-5-yl)-1-(pyridin-3-yl)pyridazin-4(1H)-one at 0° C., and the mixture was stirred overnight at room temperature. The precipitated solid was collected by filtration to give the title compound (168 mg).

Provenance & Evidence