HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 89534508, compound → HCID 117647860, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 89534508 | HCID 89534508 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 117647860 | HCID 117647860 | — |
Reaction Steps
0.71 g (28% by weight) of palladium on carbon at 10% was added to a solution of 2.52 g of methyl (S)-1-(2,6-difluoro-3-nitrobenzoyl)pyrrolidine-2-carboxylate under nitrogen. The reaction medium was stirred under a hydrogen atmosphere for 2 hours. The reaction medium was filtered through celite and concentrated. The residue was used as it is in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09090596B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-37aa1837edfe482c9c69b8c5c288cc1c |
| Source note | uspto-grants-2015_07 |