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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1528207Generated: November 3, 2026

HCID 89534508, compound → HCID 117647860, compound

https://huagongshe.com/reaction/1528207

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 89534508HCID 89534508—
CatalystPalladiumHCID 23938—
ProductHCID 117647860HCID 117647860—

Reaction Steps

0.71 g (28% by weight) of palladium on carbon at 10% was added to a solution of 2.52 g of methyl (S)-1-(2,6-difluoro-3-nitrobenzoyl)pyrrolidine-2-carboxylate under nitrogen. The reaction medium was stirred under a hydrogen atmosphere for 2 hours. The reaction medium was filtered through celite and concentrated. The residue was used as it is in the next step.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09090596B2
Source datasetuspto-grants-2015_07
ORD IDord-37aa1837edfe482c9c69b8c5c288cc1c
Source noteuspto-grants-2015_07