HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 66578050, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 66578095 | HCID 66578095 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 66578050 | HCID 66578050 | — |
Reaction Steps
m-Chloroperbenzoic acid (0.024 g, 0.11 mmol) was added to a solution of 1-[4′-(4-benzylsulfanylmethyl-3-methyl-isoxazol-5-yl)-biphenyl-4-yl]-cyclopropanecarboxylic acid (0.050 g, 0.11 mmol) in CH2Cl2. After stirring for 15 minutes the mixture was concentrated and the residue was purified by preparative HPLC to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09090573B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-d3da5a78cbfd4747bc958b0d1a83541c |
| Source note | uspto-grants-2015_07 |