HRID1528779

反应详情

EQUATION

反应方程式

HRID 1528779 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

m-Chloroperbenzoic acid (0.023 g, 0.11 mmol) was added to a solution of 1-[4′-(3-methyl-4-phenethylsulfanylmethyl-isoxazol-5-yl)-biphenyl-4-yl]-cyclopropanecarboxylic acid (0.050 g, 0.11 mmol) in CH2Cl2. After stirring for 15 minutes the mixture was concentrated and the residue was purified by preparative HPLC to give the title compound.

WORKUP

后处理

  1. concentrationwas concentrated
  2. customthe residue was purified by preparative HPLC