Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | 4-Bromomethyl-5-(4-bromo-phenyl)-3-methyl-isoxazole | HCID 66577223 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86673637 | HCID 86673637 | — |
Reaction Steps
To 4-bromomethyl-5-(4-bromo-phenyl)-3-methyl-isoxazole (3.68 g, 11.12 mmol) in DMF (30 mL) was added sodium azide (1.83 g, 27.79 mmol) and the reaction was stirred at 80° C. for 1 hour. After aqueous workup, the mixture was concentrated to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09090573B2 |
|---|
| Source dataset | uspto-grants-2015_07 |
|---|
| ORD ID | ord-4e98d64a7f76473a9905c714a6ee1f98 |
|---|
| Source note | uspto-grants-2015_07 |
|---|
