Benzyl chloroformate → HCID 66578238, compound
Reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[O:12][N:11]=[C:10]([CH3:13])[C:9]=2[CH2:14][NH2:15])=[CH:4][CH:3]=1.Cl[C:17]([O:19][CH2:20][C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1)=[O:18]>>[CH2:20]([O:19][C:17](=[O:18])[NH:15][CH2:14][C:9]1[C:10]([CH3:13])=[N:11][O:12][C:8]=1[C:5]1[CH:4]=[CH:3][C:2]([Br:1])=[CH:7][CH:6]=1)[C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1Participants
3
Procedure
Prepared according to the procedure described in Example 3, Step 7, using C-[5-(4-bromo-phenyl)-3-methyl-isoxazol-4-yl]-methylamine and benzyl chloroformate.
Workup
- customPrepared
Sources & evidence
- ORD record
- ord-7afbf3378bbb4e0584956381d4e37de0
- Source dataset
- uspto-grants-2015_07
- Patent number
- US09090573B2
Reaction notes
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